Trace analysis for aluminum by furnace atomic absorption spectroscopy and differential pulse polarography

Trace Determination of Azathioprine by Differential Pulse Polarography

A simple and rapid differential pulse polarographic method was developed for the trace determination of azathioprine. A welldefined polarogram with three peaks was obtained in acetate buffer (pH 5.0) with peak potentials -0.27 V, -0.73 V and -1.02 V. The current-concentration linearity was found extend up to 5 x 10 mol L (r = 0.9992) with minimum detection limit of 2.8x10 mol L. The values of r...

Selective Determination of Trace-Bismuth by Extraction-Differential Pulse Polarography in Non-Aqueous Media

The voltammetric characteristics of bismuth(III)-oxinate in chloroform at the mercury electrode were investigated and a quasi-reversible behavior for Bi(III) oxinate reduction was confirmed. Preceded by the extraction of Bi(III) oxinate in chloroform, differential pulse polarography was developed in the extracts for determination of the trace-bismuth. The linear range of the calibration gra...

The Analysis of Trace Elements in Honey by Flame and Graphite Furnace Atomic Absorption Spectrometry

Determination of aluminum in bone by atomic absorption spectroscopy.

In developing this method for determination of Al in bone we paid special attention to the homogenization of bone samples, which presents great difficulties for trace-element analysis. To minimize the risk of contamination, we preferred low-temperature ashing over classical wet-digestion techniques for destruction of the organic material. Graphite-furnace atomic absorption spectroscopy is used ...

Aluminum determined in plasma and urine by atomic absorption spectroscopy with a transversely heated graphite atomizer furnace.

We compared a stabilized-temperature L'vov platform furnace containing an end-heated graphite atomizer (HGA) and transverse Zeeman background-correction system with a side-heated furnace system (transversely heated graphite atomizer; THGA) containing a longitudinal Zeeman background-correction system for the determination of aluminum in plasma and urine. The regression statistics for the correl...